Information card for entry 7021410

Structure parameters

• Formula: C71 H80 Cu4 N20 O31 Tb2 W2
• Calculated formula: C71 H77 Cu4 N20 O31 Tb2 W2
• Title of publication: Assembling 1D magnetic chain based on octacyanotungstate(v) and [Cu2L2Ln] sub-building units (Ln = Eu, Gd, Tb and Dy).
• Authors of publication: Song, Xiao-Jiao; Zhang, Zai-Chao; Xu, Yong-Lu; Wang, Jun; Zhou, Hong-Bo; Song, You
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 26
• Pages of publication: 9505 - 9512
• a: 9.7851 ± 0.0009 Å
• b: 12.907 ± 0.0012 Å
• c: 17.8866 ± 0.0017 Å
• α: 95.714 ± 0.001°
• β: 98.476 ± 0.001°
• γ: 104.813 ± 0.001°
• Cell volume: 2137.7 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0545
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0817
• Weighted residual factors for all reflections included in the refinement: 0.0897
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No