Information card for entry 7021563

Structure parameters

• Common name: Complex 5
• Formula: C37 H44 B N6 Ni Si
• Calculated formula: C37 H44 B N6 Ni Si
• Title of publication: Synthesis and characterization of coordinatively unsaturated nickel(ii) and manganese(ii) alkyl complexes supported by the hydrotris(3-phenyl-5-methylpyrazolyl)borate (Tp(Ph,Me)) ligand.
• Authors of publication: Abubekerov, Mark; Gianetti, Thomas L.; Kunishita, Atsushi; Arnold, John
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 29
• Pages of publication: 10525 - 10532
• a: 12.3893 ± 0.0009 Å
• b: 12.8526 ± 0.0009 Å
• c: 14.1272 ± 0.001 Å
• α: 94.844 ± 0.001°
• β: 111.526 ± 0.001°
• γ: 117.125 ± 0.001°
• Cell volume: 1774.3 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0852
• Weighted residual factors for all reflections included in the refinement: 0.0883
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No