Information card for entry 7021606

Structure parameters

• Formula: C21 H27 N6 O10 V
• Calculated formula: C21 H22 N6 O10 V
• Title of publication: Vanadium complexes having [VO](2+), [VO](3+) and [VO2](+) cores with hydrazones of 2,6-diformyl-4-methylphenol: synthesis, characterization, reactivity, and catalytic potential.
• Authors of publication: Maurya, Mannar R.; Haldar, Chanchal; Kumar, Amit; Kuznetsov, Maxim L.; Avecilla, Fernando; Costa Pessoa, João
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 33
• Pages of publication: 11941 - 11962
• a: 16.115 ± 0.005 Å
• b: 12.857 ± 0.005 Å
• c: 23.586 ± 0.005 Å
• α: 90 ± 0.005°
• β: 90 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 4887 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0832
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for significantly intense reflections: 0.138
• Weighted residual factors for all reflections included in the refinement: 0.1578
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No