Information card for entry 7021617

Structure parameters

• Formula: C66 H75 Ag2 B2 F8 N5 O P4 S2
• Calculated formula: C66 H75 Ag2 B2 F8 N5 O P4 S2
• Title of publication: Influence of a thioether function in short-bite diphosphine ligands on the nature of their silver complexes: structure of a trinuclear complex and of a coordination polymer.
• Authors of publication: Rosa, Vitor; Fliedel, Christophe; Ghisolfi, Alessio; Pattacini, Roberto; Avilés, Teresa; Braunstein, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 34
• Pages of publication: 12109 - 12119
• a: 14.0539 ± 0.0004 Å
• b: 15.7062 ± 0.0005 Å
• c: 17.3266 ± 0.0004 Å
• α: 85.636 ± 0.002°
• β: 66.492 ± 0.002°
• γ: 81.586 ± 0.002°
• Cell volume: 3468.73 ± 0.18 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0832
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for significantly intense reflections: 0.123
• Weighted residual factors for all reflections included in the refinement: 0.1425
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No