Condensed, solution and gas phase behaviour of mono- and dinuclear 2,6-diacetylpyridine (dap) hydrazone copper complexes probed by X-ray, mass spectrometry and theoretical calculations.
Authors of publication
Neto, Brenno A. D.; Viana, Barbara F. L.; Rodrigues, Thyago S.; Lalli, Priscila M.; Eberlin, Marcos N.; da Silva, Wender A.; de Oliveira, Heibbe C. B.; Gatto, Claudia C.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2013
Journal volume
42
Journal issue
32
Pages of publication
11497 - 11506
a
20.987 ± 0.0004 Å
b
18.809 ± 0.0003 Å
c
15.3539 ± 0.0003 Å
α
90°
β
113.536 ± 0.001°
γ
90°
Cell volume
5556.66 ± 0.18 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
5
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0788
Residual factor for significantly intense reflections
0.0609
Weighted residual factors for significantly intense reflections
0.1587
Weighted residual factors for all reflections included in the refinement
0.1714
Goodness-of-fit parameter for all reflections included in the refinement
