Information card for entry 7021730

Structure parameters

• Formula: C88 H92 Dy Li N4 O4 P4
• Calculated formula: C88 H92 Dy Li N4 O4 P4
• Title of publication: Slow magnetic relaxation in tris(diphosphanylamido) and tetra(phosphanoamido) dysprosium complexes.
• Authors of publication: Völcker, Franziska; Lan, Yanhua; Powell, Annie K.; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 32
• Pages of publication: 11471 - 11475
• a: 14.953 ± 0.003 Å
• b: 24.603 ± 0.005 Å
• c: 26.133 ± 0.005 Å
• α: 90°
• β: 103.96 ± 0.03°
• γ: 90°
• Cell volume: 9330 ± 3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1085
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for significantly intense reflections: 0.0617
• Weighted residual factors for all reflections included in the refinement: 0.0722
• Goodness-of-fit parameter for all reflections included in the refinement: 0.742
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No