Information card for entry 7021886

Structure parameters

• Formula: C18 H133 K3 La6 Mn3 N3 O185 S2 V39
• Calculated formula: C18 K3 La6 Mn3 N3 O170 S2 V39
• Title of publication: Assembly of trimeric polyoxovanadate aggregates based on [MnV13O38](7-) building blocks and lanthanide cations.
• Authors of publication: Liu, Ding; Lu, Ying; Li, Yang-Guang; Tan, Hua-Qiao; Chen, Wei-Lin; Zhang, Zhi-Ming; Wang, En-Bo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 40
• Pages of publication: 14445 - 14453
• a: 24.559 ± 0.003 Å
• b: 24.559 ± 0.003 Å
• c: 17.082 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 8922.6 ± 1.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 9
• Space group number: 176
• Hermann-Mauguin space group symbol: P 63/m
• Hall space group symbol: -P 6c
• Residual factor for all reflections: 0.0758
• Residual factor for significantly intense reflections: 0.0502
• Weighted residual factors for significantly intense reflections: 0.1304
• Weighted residual factors for all reflections included in the refinement: 0.1415
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No