The synthesis, spectroscopy and X-ray single crystal structure of catena-[(μ-anacardato)-copper(ii)bipyridine][Cu2{(μ-O2CC6H3(o-OH)(o-C15H31)}4(NC5H5)2].
Authors of publication
Malik, Mohammad Azad; O'Brien, Paul; Tuna, Floriana; Pritchard, Robin; Buchweishaija, Joseph; Kimambo, Elianaso; Mubofu, Egid B.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2013
Journal volume
42
Journal issue
40
Pages of publication
14438 - 14444
a
10.8423 ± 0.0005 Å
b
11.7031 ± 0.0007 Å
c
19.1273 ± 0.0013 Å
α
94.023 ± 0.002°
β
92.903 ± 0.002°
γ
104.049 ± 0.002°
Cell volume
2342.9 ± 0.2 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.19
Residual factor for significantly intense reflections
0.1002
Weighted residual factors for significantly intense reflections
0.2138
Weighted residual factors for all reflections included in the refinement
0.2704
Goodness-of-fit parameter for all reflections included in the refinement