Information card for entry 7022007

Structure parameters

• Formula: C40 H54 I N4 O Yb
• Calculated formula: C40 H54 I N4 O Yb
• Title of publication: Divalent europium and ytterbium complexes supported by a bulky 2-pyridyl amido ligand: synthesis, structure and reactivity studies.
• Authors of publication: Ku, Ka Wai; Au, Chi Wai; Chan, Hoi-Shan; Lee, Hung Kay
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 8
• Pages of publication: 2841 - 2852
• a: 19.2421 ± 0.0005 Å
• b: 12.6237 ± 0.0003 Å
• c: 17.8425 ± 0.0004 Å
• α: 90°
• β: 100.408 ± 0.001°
• γ: 90°
• Cell volume: 4262.75 ± 0.18 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.03
• Residual factor for significantly intense reflections: 0.0253
• Weighted residual factors for significantly intense reflections: 0.0629
• Weighted residual factors for all reflections included in the refinement: 0.0647
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No