Oligo-nuclear silver thiocyanate complexes with monodentate tertiary phosphine ligands, including novel 'cubane' and 'step' tetramer forms of AgSCN : PR3 (1:1)4.
Authors of publication
Bowmaker, Graham A.; Di Nicola, Corrado; Effendy,; Hanna, John V.; Healy, Peter C.; King, Scott P.; Marchetti, Fabio; Pettinari, Claudio; Robinson, Ward T.; Skelton, Brian W.; Sobolev, Alexandre N.; Tăbăcaru, Aurel; White, Allan H.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2013
Journal volume
42
Journal issue
1
Pages of publication
277 - 291
a
13.358 ± 0.0012 Å
b
14.0634 ± 0.0013 Å
c
14.2421 ± 0.0012 Å
α
88.369 ± 0.002°
β
78.086 ± 0.002°
γ
82.16 ± 0.002°
Cell volume
2593.4 ± 0.4 Å3
Cell temperature
300 ± 2 K
Ambient diffraction temperature
300 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0616
Residual factor for significantly intense reflections
0.0464
Weighted residual factors for significantly intense reflections
0.125
Weighted residual factors for all reflections included in the refinement
0.1381
Goodness-of-fit parameter for all reflections included in the refinement
