Oligo-nuclear silver thiocyanate complexes with monodentate tertiary phosphine ligands, including novel 'cubane' and 'step' tetramer forms of AgSCN : PR3 (1:1)4.
Authors of publication
Bowmaker, Graham A.; Di Nicola, Corrado; Effendy,; Hanna, John V.; Healy, Peter C.; King, Scott P.; Marchetti, Fabio; Pettinari, Claudio; Robinson, Ward T.; Skelton, Brian W.; Sobolev, Alexandre N.; Tăbăcaru, Aurel; White, Allan H.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2013
Journal volume
42
Journal issue
1
Pages of publication
277 - 291
a
13.2746 ± 0.0011 Å
b
13.7113 ± 0.0011 Å
c
14.2718 ± 0.0012 Å
α
85.26 ± 0.001°
β
88.87 ± 0.001°
γ
78.721 ± 0.001°
Cell volume
2538.7 ± 0.4 Å3
Cell temperature
300 ± 2 K
Ambient diffraction temperature
300 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.063
Residual factor for significantly intense reflections
0.0415
Weighted residual factors for significantly intense reflections
0.0983
Weighted residual factors for all reflections included in the refinement
0.1063
Goodness-of-fit parameter for all reflections included in the refinement
