Crystallography Open Database

Information card for entry 7022172

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Coordinates	7022172.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H20 Cu3 N20 O46 Si W12
Calculated formula	C24 H20 Cu3 N20 O46 Si W12
Title of publication	Secondary spacer modulated assembly of polyoxometalate based metal-organic frameworks.
Authors of publication	Sha, Jing-Quan; Sun, Jing-Wen; Li, Meng-Ting; Wang, Cheng; Li, Guang-Ming; Yan, Peng-Fei; Sun, Long-Jiang
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	5
Pages of publication	1667 - 1677
a	22.69 ± 0.006 Å
b	13.916 ± 0.004 Å
c	20.317 ± 0.005 Å
α	90°
β	98.975 ± 0.004°
γ	90°
Cell volume	6337 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1856
Residual factor for significantly intense reflections	0.1256
Weighted residual factors for significantly intense reflections	0.2342
Weighted residual factors for all reflections included in the refinement	0.2586
Goodness-of-fit parameter for all reflections included in the refinement	1.124
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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