Information card for entry 7022186

Structure parameters

• Formula: C19 H36 Al Cl2 N3
• Calculated formula: C19 H36 Al Cl2 N3
• SMILES: C1CCCCC1N1[Al](Cl)([N](C2CCCCC2)=C1N(C(C)C)C(C)C)Cl
• Title of publication: Salt metathesis for the synthesis of M-Al and M-H-Al bonds.
• Authors of publication: Riddlestone, Ian M.; Urbano, Juan; Phillips, Nicholas; Kelly, Michael J.; Vidovic, Dragoslav; Bates, Joshua I.; Taylor, Russell; Aldridge, Simon
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 1
• Pages of publication: 249 - 258
• a: 18.7208 ± 0.0008 Å
• b: 10.1409 ± 0.0004 Å
• c: 12.0592 ± 0.0006 Å
• α: 90°
• β: 91.8321 ± 0.0019°
• γ: 90°
• Cell volume: 2288.22 ± 0.18 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0507
• Residual factor for significantly intense reflections: 0.0405
• Weighted residual factors for all reflections: 0.1077
• Weighted residual factors for significantly intense reflections: 0.1023
• Weighted residual factors for all reflections included in the refinement: 0.1077
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9841
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No