Information card for entry 7022222

Structure parameters

• Formula: C22 H24 Ag B F4 N10 O6
• Calculated formula: C22 H24 Ag B F4 N10 O6
• SMILES: [Ag]12([N](O)=C(c3[n]1c1C(=O)N(C)C(=O)N(c1nc3C)C)C)[n]1c3c(nc(C)c1C(=[N]2O)C)N(C(=O)N(C3=O)C)C.[B](F)(F)(F)[F-]
• Title of publication: Heteropolyhedral silver compounds containing the polydentate ligand N,N,O-E-[6-(hydroxyimino)ethyl]-1,3,7-trimethyllumazine. Preparation, spectral and XRD structural study and AIM calculations.
• Authors of publication: Jiménez-Pulido, Sonia B; Hueso-Ureña, Francisco; Fernández-Liencres, M Paz; Fernández-Gómez, Manuel; Moreno-Carretero, Miguel N
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 2
• Pages of publication: 530 - 541
• a: 16.493 ± 0.003 Å
• b: 9.5635 ± 0.0006 Å
• c: 17.306 ± 0.003 Å
• α: 90°
• β: 97.588 ± 0.015°
• γ: 90°
• Cell volume: 2705.8 ± 0.7 ų
• Cell temperature: 77 ± 2 K
• Ambient diffraction temperature: 77 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1642
• Residual factor for significantly intense reflections: 0.0731
• Weighted residual factors for significantly intense reflections: 0.1816
• Weighted residual factors for all reflections included in the refinement: 0.2468
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No