Information card for entry 7022277

Structure parameters

• Formula: C24 H58 K Li2 N5
• Calculated formula: C24 H58 K Li2 N5
• Title of publication: A hetero-alkali-metal version of the utility amide LDA: lithium-potassium diisopropylamide.
• Authors of publication: Armstrong, David R.; Kennedy, Alan R.; Mulvey, Robert E.; Robertson, Stuart D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 10
• Pages of publication: 3704 - 3711
• a: 15.7304 ± 0.0008 Å
• b: 13.4168 ± 0.0005 Å
• c: 16.7662 ± 0.001 Å
• α: 90°
• β: 116.115 ± 0.007°
• γ: 90°
• Cell volume: 3177.3 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.057
• Residual factor for significantly intense reflections: 0.0454
• Weighted residual factors for significantly intense reflections: 0.1147
• Weighted residual factors for all reflections included in the refinement: 0.1231
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No