Information card for entry 7022379

Structure parameters

• Formula: C76 H88 N4 S Sb2
• Calculated formula: C76 H88 N4 S Sb2
• SMILES: c1(c(cccc1)/C=N/c1c(cccc1C(C)C)C(C)C)[Sb](S[Sb](c1c(cccc1)/C=N/c1c(cccc1C(C)C)C(C)C)c1c(cccc1)/C=N/c1c(cccc1C(C)C)C(C)C)c1c(cccc1)/C=N/c1c(cccc1C(C)C)C(C)C
• Title of publication: Organoantimony(III) compounds containing (imino)aryl ligands of the type 2-(RN=CH)C6H4 (R = 2',4',6'-Me3C6H2, 2',6'-(i)Pr2C6H3): bromides and chalcogenides.
• Authors of publication: Preda, Ana Maria; Raţ, Ciprian I; Silvestru, Cristian; Breunig, Hans J.; Lang, Heinrich; Rüffer, Tobias; Mehring, Michael
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 4
• Pages of publication: 1144 - 1158
• a: 30.526 ± 0.0015 Å
• b: 10.5847 ± 0.0004 Å
• c: 22.4533 ± 0.0013 Å
• α: 90°
• β: 109.267 ± 0.006°
• γ: 90°
• Cell volume: 6848.5 ± 0.6 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0251
• Weighted residual factors for significantly intense reflections: 0.0583
• Weighted residual factors for all reflections included in the refinement: 0.0598
• Goodness-of-fit parameter for all reflections included in the refinement: 0.929
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No