Information card for entry 7022384

Structure parameters

• Formula: C43.25 H45 N2 O5.25 S2 Sb2 W
• Calculated formula: C43.25 H45 N2 O5.25 S2 Sb2 W
• Title of publication: Organoantimony(III) compounds containing (imino)aryl ligands of the type 2-(RN=CH)C6H4 (R = 2',4',6'-Me3C6H2, 2',6'-(i)Pr2C6H3): bromides and chalcogenides.
• Authors of publication: Preda, Ana Maria; Raţ, Ciprian I; Silvestru, Cristian; Breunig, Hans J.; Lang, Heinrich; Rüffer, Tobias; Mehring, Michael
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 4
• Pages of publication: 1144 - 1158
• a: 12.2021 ± 0.0005 Å
• b: 14.1285 ± 0.0005 Å
• c: 14.3583 ± 0.0005 Å
• α: 82.67 ± 0.003°
• β: 74.98 ± 0.003°
• γ: 69.615 ± 0.003°
• Cell volume: 2239.13 ± 0.15 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0353
• Residual factor for significantly intense reflections: 0.0233
• Weighted residual factors for significantly intense reflections: 0.0437
• Weighted residual factors for all reflections included in the refinement: 0.0447
• Goodness-of-fit parameter for all reflections included in the refinement: 0.918
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No