Information card for entry 7022404

Structure parameters

• Common name: [Cu(bedmpza)(N3)2]2.2(ClO4)
• Formula: C28 H46 Cl2 Cu2 N16 O8
• Calculated formula: C28 H46 Cl2 Cu2 N16 O8
• Title of publication: Metal ions directing the geometry and nuclearity of azido-metal(II) complexes derived from bis(2-(3,5-dimethyl-1H-pyrazol-1-yl)ethyl)amine.
• Authors of publication: Massoud, Salah S.; Louka, Febee R.; Obaid, Yasser K.; Vicente, Ramon; Ribas, Joan; Fischer, Roland C.; Mautner, Franz A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 11
• Pages of publication: 3968 - 3978
• a: 18.9947 ± 0.001 Å
• b: 21.838 ± 0.0012 Å
• c: 20.7195 ± 0.0011 Å
• α: 90°
• β: 110.143 ± 0.002°
• γ: 90°
• Cell volume: 8068.9 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for significantly intense reflections: 0.0957
• Weighted residual factors for all reflections included in the refinement: 0.1073
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No