Information card for entry 7022428

Structure parameters

• Common name: Mo(dpma-mes)(NMe2)2(tBuNC)
• Formula: C42 H64 Mo N6 O
• Calculated formula: C42 H64 Mo N6 O
• Title of publication: Single-site N-N bond cleavage by Mo(IV): possible mechanisms of hydrazido(1-) to nitrido conversion.
• Authors of publication: DiFranco, Stephen A.; Staples, Richard J.; Odom, Aaron L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 7
• Pages of publication: 2530 - 2539
• a: 11.1614 ± 0.0002 Å
• b: 30.3369 ± 0.0007 Å
• c: 12.4226 ± 0.0003 Å
• α: 90°
• β: 98.527 ± 0.002°
• γ: 90°
• Cell volume: 4159.82 ± 0.16 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0587
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.084
• Weighted residual factors for all reflections included in the refinement: 0.0913
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No