Information card for entry 7022508

Structure parameters

• Formula: C71 H77 B F20 N3 O3 Si2 Y
• Calculated formula: C71 H77 B F20 N3 O3 Si2 Y
• SMILES: [Y]1(N([SiH](C)C)[SiH](C)C)([O]2CCCC2)([O]2CCCC2)([O]2CCCC2)[N](=C(N1c1c(cccc1C(C)C)C(C)C)c1ccccc1)c1c(cccc1C(C)C)C(C)C.Fc1c(c(F)c(F)c(F)c1F)[B-](c1c(F)c(F)c(F)c(F)c1F)(c1c(F)c(F)c(F)c(F)c1F)c1c(F)c(F)c(F)c(F)c1F
• Title of publication: Synthesis of mono-amidinate-ligated rare-earth-metal bis(silylamide) complexes and their reactivity with [Ph3C][B(C6F5)4], AlMe3 and isoprene.
• Authors of publication: Luo, Yunjie; Lei, Yinlin; Fan, Shimin; Wang, Yibin; Chen, Jue
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 11
• Pages of publication: 4040 - 4051
• a: 21.1633 ± 0.0016 Å
• b: 12.3731 ± 0.0009 Å
• c: 27.746 ± 0.002 Å
• α: 90°
• β: 96.515 ± 0.003°
• γ: 90°
• Cell volume: 7218.5 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1395
• Residual factor for significantly intense reflections: 0.0976
• Weighted residual factors for significantly intense reflections: 0.1468
• Weighted residual factors for all reflections included in the refinement: 0.1608
• Goodness-of-fit parameter for all reflections included in the refinement: 1.158
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No