Information card for entry 7022555

Structure parameters

• Formula: C142.65 H116.31 B8 Cl19.31 Co4 F32 N25 O17 S8
• Calculated formula: C141.655 H114.31 B8 Cl17.31 Co4 F32 N25 O17 S8
• Title of publication: Synthesis of ligands containing N-oxide donor atoms and their assembly into metallosupramolecular structures.
• Authors of publication: Bullock, Samantha J.; Harding, Lindsay P.; Moore, Michelle P.; Mills, Andrew; Piela, Sean A. F.; Rice, Craig R.; Towns-Andrews, Liz; Whitehead, Martina
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 16
• Pages of publication: 5805 - 5811
• a: 17.9775 ± 0.0015 Å
• b: 21.8535 ± 0.0018 Å
• c: 24.415 ± 0.002 Å
• α: 105.483 ± 0.002°
• β: 95.76 ± 0.002°
• γ: 103.275 ± 0.002°
• Cell volume: 8862.2 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1574
• Residual factor for significantly intense reflections: 0.0925
• Weighted residual factors for significantly intense reflections: 0.2724
• Weighted residual factors for all reflections included in the refinement: 0.3036
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No