Information card for entry 7022613

Structure parameters

• Common name: compound3a
• Formula: C22 H30 O8 Ru3 Si3
• Calculated formula: C22 H30 O8 Ru3 Si3
• Title of publication: Coupling of acetylene molecules on ruthenium clusters, involving cleavage of C-Si bonds in the alkyne and coordination of a phenyl ring of a SiPh3 group.
• Authors of publication: González-López, Vianney; Leyva, Marco A.; Rosales-Hoz, María J
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 15
• Pages of publication: 5401 - 5411
• a: 9.2297 ± 0.0006 Å
• b: 18.2204 ± 0.0013 Å
• c: 18.5059 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3112.1 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1421
• Residual factor for significantly intense reflections: 0.0697
• Weighted residual factors for significantly intense reflections: 0.0948
• Weighted residual factors for all reflections included in the refinement: 0.1147
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No