Information card for entry 7022671

Structure parameters

• Formula: C73 H76 Gd4 N12 O29
• Calculated formula: C73 H76 Gd4 N12 O29
• Title of publication: Polynuclear lanthanide (Ln) complexes of a tri-functional hydrazone ligand–mononuclear (Dy), dinuclear (Yb, Tm), tetranuclear (Gd), and hexanuclear (Gd, Dy, Tb) examples.
• Authors of publication: Anwar, Muhammad U.; Dawe, Louise N.; Tandon, Santokh S.; Bunge, Scott D.; Thompson, Laurence K.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 21
• Pages of publication: 7781 - 7794
• a: 12.845 ± 0.005 Å
• b: 13.379 ± 0.006 Å
• c: 15.046 ± 0.007 Å
• α: 74.15 ± 0.02°
• β: 66.72 ± 0.02°
• γ: 64.47 ± 0.02°
• Cell volume: 2126.7 ± 1.7 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1041
• Residual factor for significantly intense reflections: 0.0825
• Weighted residual factors for significantly intense reflections: 0.2392
• Weighted residual factors for all reflections included in the refinement: 0.3015
• Goodness-of-fit parameter for all reflections included in the refinement: 1.199
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No