Information card for entry 7022709

Structure parameters

• Formula: C32 H52 Cl N6 O2 Yb
• Calculated formula: C32 H52 Cl N6 O2 Yb
• SMILES: C1(=[N]2c3cccc4c3c(ccc4)N3[Yb]2(N1C(C)C)([O]1CCCC1)(Cl)([N](C(C)C)=C3NC(C)C)[O]1CCCC1)NC(C)C
• Title of publication: Unprecedented reaction of bridged bis(guanidinate) lanthanide complexes: sterically induced deprotonation.
• Authors of publication: Wang, Chuanyong; Zhang, Xingmin; Xue, Mingqiang; Zhang, Yong; Shen, Qi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 19
• Pages of publication: 7009 - 7018
• a: 13.8453 ± 0.0006 Å
• b: 12.2986 ± 0.0004 Å
• c: 20.3408 ± 0.0009 Å
• α: 90°
• β: 93.541 ± 0.004°
• γ: 90°
• Cell volume: 3457 ± 0.2 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.038
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.0756
• Weighted residual factors for all reflections included in the refinement: 0.0777
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No