Information card for entry 7022772

Structure parameters

• Chemical name: bisaqua-1,4,7,10,13,16-hexaoxacyclooctadecane-lead(II) bis(hexafluorophosphate) hydrate
• Formula: C12 H28.4 F12 O8.2 P2 Pb
• Calculated formula: C12 H24 F12 O8.2 P2 Pb
• Title of publication: Lead(II) tetrafluoroborate and hexafluorophosphate complexes with crown ethers, mixed O/S- and O/Se-donor macrocycles and unusual [BF(4)](-) and [PF(6)](-) coordination.
• Authors of publication: Farina, Paolo; Latter, Thomas; Levason, William; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 13
• Pages of publication: 4714 - 4724
• a: 8.754 ± 0.003 Å
• b: 15.23 ± 0.004 Å
• c: 9.254 ± 0.003 Å
• α: 90°
• β: 91.453 ± 0.006°
• γ: 90°
• Cell volume: 1233.4 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0756
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for significantly intense reflections: 0.1411
• Weighted residual factors for all reflections included in the refinement: 0.15
• Goodness-of-fit parameter for all reflections included in the refinement: 1.108
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No