Rare-earth dichloro and bis(alkyl) complexes supported by bulky amido-imino ligand. Synthesis, structure, reactivity and catalytic activity in isoprene polymerization.
Authors of publication
Kissel, Alexander A.; Lyubov, Dmitry M.; Mahrova, Tatyana V.; Fukin, Georgy K.; Cherkasov, Anton V.; Glukhova, Tatyana A.; Cui, Dongmei; Trifonov, Alexander A.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2013
Journal volume
42
Journal issue
25
Pages of publication
9211 - 9225
a
13.6998 ± 0.0007 Å
b
17.3673 ± 0.0009 Å
c
15.5199 ± 0.0008 Å
α
90°
β
90.248 ± 0.001°
γ
90°
Cell volume
3692.6 ± 0.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.075
Residual factor for significantly intense reflections
0.0513
Weighted residual factors for significantly intense reflections
0.115
Weighted residual factors for all reflections included in the refinement
0.125
Goodness-of-fit parameter for all reflections included in the refinement
