Information card for entry 7022993

Structure parameters

• Common name: bis(mu!3$-1,2-dithiolatoethane-S,S,S',S')-diethanido - tris(triisopropylphosphine)-tricopper(+1)-gallium(+3)
• Chemical name: bis(μ~3~-1,2-dithiolatoethane-S,S,S',S')-diethanido -tris(triisopropylphosphine)-tricopper(+1)-gallium(+3)
• Formula: C35 H81 Cu3 Ga P3 S4
• Calculated formula: C35 H81 Cu3 Ga P3 S4
• Title of publication: Tetranuclear organometallic complexes based on 1,2-ethanedithiolate ligands as potential precursors for CuMS2 (M = Ga, In).
• Authors of publication: Friedrich, Dirk; Kluge, Oliver; Kischel, Marcus; Krautscheid, Harald
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 26
• Pages of publication: 9613 - 9620
• a: 13.5627 ± 0.0011 Å
• b: 13.9556 ± 0.0011 Å
• c: 16.0504 ± 0.0014 Å
• α: 64.19 ± 0.006°
• β: 68.597 ± 0.007°
• γ: 66.96 ± 0.006°
• Cell volume: 2446.4 ± 0.4 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0706
• Weighted residual factors for all reflections included in the refinement: 0.0745
• Goodness-of-fit parameter for all reflections included in the refinement: 0.94
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No