Information card for entry 7023217

Structure parameters

• Formula: C54 H43 B2 F8 N8 O4 Pd3
• Calculated formula: C54 H35 B2 F8 N8 O4 Pd3
• Title of publication: Trinuclear palladium addition to unsaturated carbocycles.
• Authors of publication: Murahashi, Tetsuro; Takase, Kohei; Usui, Kentaro; Kimura, Seita; Fujimoto, Mayu; Uemura, Tomohito; Ogoshi, Sensuke; Yamamoto, Koji
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 29
• Pages of publication: 10626 - 10632
• a: 16.2696 ± 0.0019 Å
• b: 16.6999 ± 0.0019 Å
• c: 22.126 ± 0.003 Å
• α: 81.787 ± 0.003°
• β: 71.232 ± 0.003°
• γ: 64.084 ± 0.003°
• Cell volume: 5119.6 ± 1.1 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0544
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No