Information card for entry 7023441

Structure parameters

• Common name: A-Ghosh sample 1
• Chemical name: Li-salt of Co(III)-dibromide complex with amidate ligand, CH3CN solvate
• Formula: C9.45 H10 Br Co0.5 Li0.5 N3.24 O
• Calculated formula: C9.182 H10 Br Co0.5 Li0.5 N3.10475 O
• Title of publication: Synthesis and characterization of Co(III) amidoamine complexes: influence of substituents of the ligand on catalytic cyclic carbonate synthesis from epoxide and carbon dioxide.
• Authors of publication: Ramidi, Punnamchandar; Gerasimchuk, Nikolay; Gartia, Yashraj; Felton, Charlette M.; Ghosh, Anindya
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 36
• Pages of publication: 13151 - 13160
• a: 9.0155 ± 0.0012 Å
• b: 17.429 ± 0.002 Å
• c: 15.794 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2481.7 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 20
• Hermann-Mauguin space group symbol: C 2 2 21
• Hall space group symbol: C 2c 2
• Residual factor for all reflections: 0.0654
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.0815
• Weighted residual factors for all reflections included in the refinement: 0.0911
• Goodness-of-fit parameter for all reflections included in the refinement: 0.989
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No