Information card for entry 7023446

Structure parameters

• Formula: C36 H24 Cu11 N54 O12
• Calculated formula: C36 H24 Cu11 N54 O12
• Title of publication: Rung-defected ladder of azido-bridged Cu(II) chains linked by [Cu(picolinate)2] units.
• Authors of publication: Liu, Jiang; Qin, Ying-Lian; Qu, Mei; Clérac, Rodolphe; Zhang, Xian-Ming
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 32
• Pages of publication: 11571 - 11575
• a: 11.05 ± 0.003 Å
• b: 12.255 ± 0.004 Å
• c: 13.652 ± 0.004 Å
• α: 94.145 ± 0.007°
• β: 106.864 ± 0.006°
• γ: 107.51 ± 0.005°
• Cell volume: 1661.3 ± 0.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1534
• Residual factor for significantly intense reflections: 0.0793
• Weighted residual factors for significantly intense reflections: 0.1708
• Weighted residual factors for all reflections included in the refinement: 0.228
• Goodness-of-fit parameter for all reflections included in the refinement: 0.98
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No