Information card for entry 7023505

Structure parameters

• Formula: C93 H176 Al6 N4 O18.75 Si8
• Calculated formula: C93 H176 Al6 N4 O18.75 Si8
• Title of publication: Synthesis of metallasiloxanes of group 13-15 and their application in catalysis.
• Authors of publication: Li, Yan; Wang, Jinjin; Wu, Yile; Zhu, Hongping; Samuel, Prinson P.; Roesky, Herbert W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 37
• Pages of publication: 13715 - 13722
• a: 18.6059 ± 0.0005 Å
• b: 18.7005 ± 0.0005 Å
• c: 35.0951 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12211 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1126
• Residual factor for significantly intense reflections: 0.0793
• Weighted residual factors for significantly intense reflections: 0.186
• Weighted residual factors for all reflections included in the refinement: 0.2045
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No