Information card for entry 7023525

Structure parameters

• Formula: C107.5 H88 Cl5 F28 N3 P10 Pd4
• Calculated formula: C107.5 H84 Cl5 F28 N3 P10 Pd4
• Title of publication: Flexible, linear, tetranuclear palladium complexes supported by tetraphosphine ligands with electron-withdrawing groups.
• Authors of publication: Tanase, Tomoaki; Hatada, Satoko; Mochizuki, Ayaka; Nakamae, Kanako; Kure, Bunsho; Nakajima, Takayuki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 45
• Pages of publication: 15941 - 15952
• a: 14.9851 ± 0.0007 Å
• b: 20.2837 ± 0.0013 Å
• c: 20.9517 ± 0.0014 Å
• α: 109.4 ± 0.003°
• β: 98.8437 ± 0.0019°
• γ: 90.3785 ± 0.0011°
• Cell volume: 5924 ± 0.6 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.094
• Weighted residual factors for all reflections included in the refinement: 0.2808
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No