Hierarchical assembly of discrete copper(II) metallo-structures from pre-assembled dinuclear (bis-β-diketonato)metallocycles and flexible difunctional co-ligands.
Authors of publication
Clegg, Jack K.; Li, Feng; Jolliffe, Katrina A.; Lindoy, Leonard F.; Meehan, George V.; Parsons, Simon; Tasker, Peter A.; White, Fraser J.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2013
Journal volume
42
Journal issue
39
Pages of publication
14315 - 14323
a
11.3608 ± 0.0009 Å
b
14.4945 ± 0.0011 Å
c
17.5171 ± 0.0013 Å
α
78.648 ± 0.001°
β
80.525 ± 0.001°
γ
79.962 ± 0.001°
Cell volume
2759.3 ± 0.4 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0462
Residual factor for significantly intense reflections
0.0333
Weighted residual factors for significantly intense reflections
0.0855
Weighted residual factors for all reflections included in the refinement
0.0925
Goodness-of-fit parameter for all reflections included in the refinement
