Information card for entry 7023887

Structure parameters

• Formula: C18 H25 Cl2 N O3 Pd Te2
• Calculated formula: C18 H25 Cl2 N O3 Pd Te2
• SMILES: [Pd]12([Te](CC[NH]2CC[Te]1c1ccc(OC)cc1)c1ccc(OC)cc1)Cl.[Cl-].O
• Title of publication: Palladium(ii)-(E,N,E) pincer ligand (E = S/Se/Te) complex catalyzed Suzuki coupling reactions in water via in situ generated palladium quantum dots.
• Authors of publication: Kumar, Satyendra; Rao, Gyandshwar K.; Kumar, Arun; Singh, Mahabir P.; Singh, Ajai Kumar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 48
• Pages of publication: 16939 - 16948
• a: 18.5 ± 0.002 Å
• b: 10.3779 ± 0.0014 Å
• c: 37.183 ± 0.005 Å
• α: 90°
• β: 98.127 ± 0.003°
• γ: 90°
• Cell volume: 7067.1 ± 1.5 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1492
• Residual factor for significantly intense reflections: 0.1153
• Weighted residual factors for significantly intense reflections: 0.1889
• Weighted residual factors for all reflections included in the refinement: 0.2014
• Goodness-of-fit parameter for all reflections included in the refinement: 1.339
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No