Information card for entry 7023894

Structure parameters

• Formula: C42 H46 N12 Ni O41 V W12
• Calculated formula: C42 H38 N12 Ni O41 V W12
• Title of publication: Two three-dimensional porous frameworks built from metal-organic coordination polymer sheets pillared by polyoxometalate clusters.
• Authors of publication: Lan, Qing; Zhang, Jun; Zhang, Zhi-Ming; Lu, Ying; Wang, En-Bo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 47
• Pages of publication: 16602 - 16607
• a: 22 ± 0.004 Å
• b: 15 ± 0.003 Å
• c: 24 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7920 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.083
• Residual factor for significantly intense reflections: 0.0671
• Weighted residual factors for significantly intense reflections: 0.169
• Weighted residual factors for all reflections included in the refinement: 0.1779
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No