Information card for entry 7023896

Structure parameters

• Formula: C20 H128 N4 Ni14 O170 P4 W30
• Calculated formula: C20 H16 N4 Ni14 O170 P4 W30
• Title of publication: Hexa-substituted polyoxometalates made of trivacant Dawson {P2W15} fragments and {Ni6} clusters under hydrothermal conditions.
• Authors of publication: Liu, Yong-Chao; Fu, Chun-Hua; Zheng, Shou-Tian; Zhao, Jun-Wei; Yang, Guo-Yu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 48
• Pages of publication: 16676 - 16679
• a: 12.853 ± 0.004 Å
• b: 14.55 ± 0.005 Å
• c: 22.905 ± 0.008 Å
• α: 86.152 ± 0.013°
• β: 82.553 ± 0.013°
• γ: 64.101 ± 0.008°
• Cell volume: 3821 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0771
• Residual factor for significantly intense reflections: 0.0548
• Weighted residual factors for significantly intense reflections: 0.1321
• Weighted residual factors for all reflections included in the refinement: 0.1473
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No