Information card for entry 7023988

Structure parameters

• Formula: C42 H44 N2 O3 Si2 Sn
• Calculated formula: C42 H44 N2 O3 Si2 Sn
• SMILES: [Sn]1(O[Si](O[Si](O1)(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(c1ccccc1)c1c(cccc1CN(C)C)CN(C)C
• Title of publication: Straightforward synthesis of novel cyclic metallasiloxanes supported by an N,C,N-chelating ligand.
• Authors of publication: Fridrichová, Adéla; Mairychová, Barbora; Padělková, Zdeňka; Lyčka, Antonín; Jurkschat, Klaus; Jambor, Roman; Dostál, Libor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 46
• Pages of publication: 16403 - 16411
• a: 10.732 ± 0.0002 Å
• b: 13.1811 ± 0.0008 Å
• c: 13.5121 ± 0.0008 Å
• α: 89.06 ± 0.005°
• β: 84.317 ± 0.004°
• γ: 87.989 ± 0.003°
• Cell volume: 1900.69 ± 0.17 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0359
• Residual factor for significantly intense reflections: 0.0266
• Weighted residual factors for significantly intense reflections: 0.0589
• Weighted residual factors for all reflections included in the refinement: 0.065
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No