Information card for entry 7025234

Structure parameters

• Formula: C49 H82 I N3 O4.5 Si3 U
• Calculated formula: C47 H78 I N3 O4 Si3 U
• SMILES: [U]12(I)(N([Si](C([Si](N1c1cc(cc(c1)C)C)(C)C)[Si](N2c1cc(cc(c1)C)C)(C)C)(C)C)c1cc(cc(c1)C)C)([O]1CCCC1)[O]1CCCC1.O1CCCC1.O1CCCC1
• Title of publication: Uranium(IV) amide and halide derivatives of two tripodal tris(N-arylamido-dimethylsilyl)methanes.
• Authors of publication: Patel, Dipti; Lewis, William; Blake, Alexander J.; Liddle, Stephen T.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 29
• Pages of publication: 6638 - 6647
• a: 12.7867 ± 0.0007 Å
• b: 12.9462 ± 0.0007 Å
• c: 18.9711 ± 0.001 Å
• α: 104.553 ± 0.002°
• β: 94.333 ± 0.002°
• γ: 114.813 ± 0.002°
• Cell volume: 2699.9 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0333
• Residual factor for significantly intense reflections: 0.0274
• Weighted residual factors for significantly intense reflections: 0.0687
• Weighted residual factors for all reflections included in the refinement: 0.0707
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No