Information card for entry 7025481

Structure parameters

• Formula: C43 H121 Ge K O4 Pb Si11
• Calculated formula: C43 H121 Ge1.0486 K O4 Pb Si10.95
• Title of publication: EPR spectroscopic characterization of persistent germyl-substituted Pb(III)- and Sn(III)-radicals.
• Authors of publication: Kurzbach, Dennis; Yao, Shenglai; Hinderberger, Dariush; Klinkhammer, Karl W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6449 - 6459
• a: 12.2196 ± 0.0008 Å
• b: 24.4992 ± 0.0016 Å
• c: 24.9634 ± 0.0015 Å
• α: 90°
• β: 99.7313 ± 0.0016°
• γ: 90°
• Cell volume: 7365.8 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0789
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.0821
• Weighted residual factors for all reflections included in the refinement: 0.088
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No