Information card for entry 7025561

Structure parameters

• Formula: C18 H35 B O2 Sm
• Calculated formula: C18 H35 B O2 Sm
• Title of publication: Synthesis of samarium(II) borohydrides and their behaviour as initiators in styrene and epsilon-caprolactone polymerisation.
• Authors of publication: Jaroschik, Florian; Bonnet, Fanny; Le Goff, Xavier-Frédéric; Ricard, Louis; Nief, François; Visseaux, Marc
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 29
• Pages of publication: 6761 - 6766
• a: 12.129 ± 0.001 Å
• b: 13.423 ± 0.001 Å
• c: 14.753 ± 0.001 Å
• α: 90°
• β: 121.69 ± 0.001°
• γ: 90°
• Cell volume: 2043.8 ± 0.3 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.0768
• Weighted residual factors for all reflections included in the refinement: 0.0918
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No