Information card for entry 7025630

Structure parameters

• Formula: C77 H107 Cl3 N4 O2 Yb2
• Calculated formula: C77 H99 Cl3 N4 O2 Yb2
• Title of publication: Controlled synthesis of mononuclear or binuclear aryloxo ytterbium complexes supported by beta-diketiminate ligand and their activity for polymerization of epsilon-caprolactone and L-lactide.
• Authors of publication: Chen, Hongxia; Liu, Peng; Yao, Haisheng; Zhang, Yong; Yao, Yingming; Shen, Qi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 29
• Pages of publication: 6877 - 6885
• a: 15.1708 ± 0.0011 Å
• b: 21.7153 ± 0.0017 Å
• c: 22.5149 ± 0.0018 Å
• α: 90°
• β: 96.893 ± 0.002°
• γ: 90°
• Cell volume: 7363.7 ± 1 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0387
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0663
• Weighted residual factors for all reflections included in the refinement: 0.0683
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No