Information card for entry 7025669

Structure parameters

• Formula: H182 K2 Na28 Ni6 O271 P6 W48
• Calculated formula: K2 Na11 Ni6 O216.35 P6 W48
• Title of publication: Understanding and mapping the assembly of a family of trimeric polyoxometalates: transition metal mediated Wells-Dawson (M18)-trimers.
• Authors of publication: Boyd, Thomas; Mitchell, Scott G.; Miras, Haralampos N.; Long, De-Liang; Cronin, Leroy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6460 - 6465
• a: 17.1003 ± 0.0003 Å
• b: 25.5173 ± 0.0004 Å
• c: 28.8698 ± 0.0005 Å
• α: 79.668 ± 0.001°
• β: 87.722 ± 0.001°
• γ: 83.463 ± 0.001°
• Cell volume: 12310.2 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0939
• Residual factor for significantly intense reflections: 0.0645
• Weighted residual factors for significantly intense reflections: 0.1778
• Weighted residual factors for all reflections included in the refinement: 0.1983
• Goodness-of-fit parameter for all reflections included in the refinement: 0.985
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No