Information card for entry 7025935

Structure parameters

• Formula: C32.67 H30.67 Cl4 O2 Pd2
• Calculated formula: C32.6667 H30.6667 Cl4 O2 Pd2
• Title of publication: PdCl(2)-promoted reactions of diaryl-substituted methylenecyclopropanes.
• Authors of publication: Qi, Ming-Hui; Shao, Li-Xiong; Shi, Min
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 37
• Pages of publication: 8829 - 8834
• a: 14.9609 ± 0.0009 Å
• b: 20.8396 ± 0.0013 Å
• c: 15.0025 ± 0.0009 Å
• α: 90°
• β: 92.076 ± 0.001°
• γ: 90°
• Cell volume: 4674.4 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0714
• Residual factor for significantly intense reflections: 0.0504
• Weighted residual factors for significantly intense reflections: 0.1373
• Weighted residual factors for all reflections included in the refinement: 0.1452
• Goodness-of-fit parameter for all reflections included in the refinement: 0.949
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No