Information card for entry 7025941

Structure parameters

• Formula: C26 H40 Cl4 N2 O2 V2
• Calculated formula: C26 H40 Cl4 N2 O2 V2
• Title of publication: Oxo- and imido-alkoxide vanadium complexes as precatalysts for the guanylation of aromatic amines.
• Authors of publication: Romero-Fernández, Javier; Carrillo-Hermosilla, Fernando; Antiñolo, Antonio; Alonso-Moreno, Carlos; Rodríguez, Ana M; López-Solera, Isabel; Otero, Antonio
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6419 - 6425
• a: 8.7453 ± 0.0019 Å
• b: 9.89 ± 0.002 Å
• c: 21.01 ± 0.005 Å
• α: 90.144 ± 0.006°
• β: 91.537 ± 0.006°
• γ: 115.928 ± 0.005°
• Cell volume: 1633.5 ± 0.6 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1281
• Residual factor for significantly intense reflections: 0.0661
• Weighted residual factors for significantly intense reflections: 0.187
• Weighted residual factors for all reflections included in the refinement: 0.2349
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No