Information card for entry 7025944

Structure parameters

• Formula: C38 H72 Cl4 P2 Ru Si2
• Calculated formula: C38 H72 Cl4 P2 Ru Si2
• Title of publication: Silyl and sigma-silane ruthenium complexes: chloride substituent effects on the catalysed silylation of ethylene.
• Authors of publication: Lachaize, Sébastien; Vendier, Laure; Sabo-Etienne, Sylviane
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 36
• Pages of publication: 8492 - 8500
• a: 9.7901 ± 0.0008 Å
• b: 44.957 ± 0.0007 Å
• c: 10.1672 ± 0.0009 Å
• α: 90°
• β: 105.977 ± 0.003°
• γ: 90°
• Cell volume: 4302.1 ± 0.5 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.133
• Residual factor for significantly intense reflections: 0.0867
• Weighted residual factors for significantly intense reflections: 0.1396
• Weighted residual factors for all reflections included in the refinement: 0.1532
• Goodness-of-fit parameter for all reflections included in the refinement: 1.137
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No