Information card for entry 7026080

Structure parameters

• Formula: C83 H104 Cl4 N4 P4 Si4 Zn2
• Calculated formula: C83 H104 Cl4 N4 P4 Si4 Zn2
• Title of publication: Bis(phosphinimino)methanides as non-innocent ligand in zinc chemistry: synthesis and structures.
• Authors of publication: Marks, Sebastian; Panda, Tarun K.; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 31
• Pages of publication: 7230 - 7235
• a: 12.585 ± 0.003 Å
• b: 16.613 ± 0.003 Å
• c: 21.407 ± 0.004 Å
• α: 84.54 ± 0.03°
• β: 82.55 ± 0.03°
• γ: 76.71 ± 0.03°
• Cell volume: 4309.1 ± 1.6 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1084
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.0946
• Weighted residual factors for all reflections included in the refinement: 0.1075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No