Information card for entry 7026162

Structure parameters

• Formula: C40 H68 Er2 N6 Si4
• Calculated formula: C40 H68 Er2 N6 Si4
• Title of publication: Rare earth metal bis(trimethylsilyl)amido complexes bearing pyrrolyl-methylamide ligand. Synthesis, structure, and catalytic activity towards guanylation of amines.
• Authors of publication: Liu, Chao; Zhou, Shuangliu; Wang, Shaowu; Zhang, Lijun; Yang, Gaosheng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 38
• Pages of publication: 8994 - 8999
• a: 12.4386 ± 0.0008 Å
• b: 14.9104 ± 0.001 Å
• c: 26.6642 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4945.3 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0638
• Residual factor for significantly intense reflections: 0.0353
• Weighted residual factors for significantly intense reflections: 0.0781
• Weighted residual factors for all reflections included in the refinement: 0.0882
• Goodness-of-fit parameter for all reflections included in the refinement: 1.237
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No