Information card for entry 7026443

Structure parameters

• Formula: C4 H32 Cu2 Mo6 N2 Na4 O42 Te
• Calculated formula: C4 H32 Cu2 Mo6 N2 Na4 O42 Te
• Title of publication: Robust 1D open rack-like architecture in coordination polymers of Anderson POMs [{Na4(H2O)14}{Cu(gly)}2][TeMo6O24] and [{Cu(en)2}3{TeW6O24}]: synthesis, characterization and heterogeneous catalytic epoxidation of olefines.
• Authors of publication: Dutta, Daipayan; Jana, Atish D.; Debnath, Mainak; Bhaumik, Asim; Marek, Jaromir; Ali, Mahammad
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 48
• Pages of publication: 11551 - 11559
• a: 7.1526 ± 0.0005 Å
• b: 10.6481 ± 0.0006 Å
• c: 14.2288 ± 0.0009 Å
• α: 73.573 ± 0.005°
• β: 78.822 ± 0.005°
• γ: 78.197 ± 0.005°
• Cell volume: 1006.74 ± 0.11 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0265
• Residual factor for significantly intense reflections: 0.0246
• Weighted residual factors for significantly intense reflections: 0.0624
• Weighted residual factors for all reflections included in the refinement: 0.0636
• Goodness-of-fit parameter for all reflections included in the refinement: 0.902
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No