Crystallography Open Database

Information card for entry 7026448

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Structure parameters

Formula	C48 H63 Cl6 N3 O0.5 P Ru
Calculated formula	C48 H63 Cl6 N3 O0.5 P Ru
Title of publication	Cyclopropanation of Ru-diimino-pyridine ligand complexes.
Authors of publication	Brown, Christopher C.; Stephan, Douglas W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	31
Pages of publication	7211 - 7213
a	12.5917 ± 0.0008 Å
b	12.8624 ± 0.0007 Å
c	15.5806 ± 0.001 Å
α	91.817 ± 0.003°
β	103.746 ± 0.004°
γ	93.184 ± 0.003°
Cell volume	2444.7 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0939
Residual factor for significantly intense reflections	0.0552
Weighted residual factors for significantly intense reflections	0.1253
Weighted residual factors for all reflections included in the refinement	0.1445
Goodness-of-fit parameter for all reflections included in the refinement	1.012
Diffraction radiation wavelength	0.71072 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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