Information card for entry 7027014

Structure parameters

• Formula: C32 H42 N2
• Calculated formula: C32 H42 N2
• Title of publication: Synthesis of some very bulky N,N′-disubstituted amidines and initial studies of their coordination chemistry †
• Authors of publication: Boeré, René T.; Klassen, Vicki; Wolmershäuser, Gotthelf
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 24
• Pages of publication: 4147
• a: 18.409 ± 0.002 Å
• b: 9.985 ± 0.001 Å
• c: 17.659 ± 0.001 Å
• α: 90°
• β: 117.13 ± 0.01°
• γ: 90°
• Cell volume: 2888.8 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1395
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.1262
• Weighted residual factors for all reflections included in the refinement: 0.1524
• Goodness-of-fit parameter for all reflections included in the refinement: 0.931
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No